Carbohydrate Analysis by Ion Chromatography

Ion Chromatography in Environmental Analysis

Quantification of carbohydrate-deficient transferrin by ion-exchange chromatography with an enzymatically prepared calibrator.

The current HPLC method for the determination of carbohydrate-deficient transferrin (CDT) yields ratios of CDT isoforms in relation to total transferrin, whereas the use of absolute concentrations obtainable in routine analysis by RIA and the reference ranges based here-upon is more convenient. We describe a modified HPLC method that likewise gives absolute CDT concentrations by using a calibra...

Off-line elimination of carbohydrates for amino acid analysis of samples with high carbohydrate content by ion-exchange chromatography.

This paper introduces a new off-line sample preparation that eliminates carbohydrates from amino acid samples containing a high carbohydrate content before analysis by anion-exchange chromatography and integrated pulsed amperometric detection. First, the sample is introduced into a cation-exchange column in the hydrogen form. Carbohydrates are removed completely using 0.02% formic acid as a tra...

The Analysis of Perchlorate by Ion Chromatography/Mass Spectrometry Application

A method for the determination of perchlorate anion at sub ppb levels using ion chromatography/mass spectrometry (IC/MS) is described. The IC/MS method follows EPA Method 314 methodology originally developed for IC with conductivity detection at the single ppb range [1]. The IC/MS method is not affected by the addition of the interference matrix described in Method 314 on perchlorate recoveries...

Ion Exclusion Chromatography: Liquid Chromatography

terials, operated in a pressure-driven mode, plotted as a function of inverse temperature. This Rgure is intended to give some appreciation of the Suxes that are attainable; however, they are not normalized to a given partial pressure gradient or thickness of membrane, and thus the Suxes are not directly comparable. Taking a value of between 10 and 100 L m 2 min 1 as the level of oxygen Sux nee...